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Início / Equipamentos / Reator de vidro / Lifting & Rotating Double-Layer Glass Reactor
SED-50BLFY-A
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SED-50BLFY-A
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SED-50BLFY-A — Lifting & Rotating Double-Layer Glass Reactor

A descrição completa deste modelo ainda está sendo traduzida. Consulte os detalhes em inglês ou solicite informações à nossa equipe. English

SED-50BLFY-A 50 L lifting and rotating double-layer glass reactor. Vessel capacity 50 L (inner diameter 365 mm, outer diameter 410 mm, inner length 576 mm); jacket capacity ~16 L. The reactor lid and all components above

Prazo de entrega
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Capacidade de produção
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Como funciona

The machine features an electrically controlled constant-speed stirring system, condenser and addition systems, and a jacket that requires connection to an external heating or cooling circulator. While stirring, hot or cold fluid is circulated through the jacket to maintain constant-temperature heating or cooling of the material inside. During heating reactions, vacuum conditions (external vacuum unit required) improve evaporation efficiency. Solvent vapour condenses in the glass condenser coil into liquid, which can either reflux back into the reactor or be recovered through the valve below the reflux elbow. When the reaction is complete, material can be discharged through the side outlet at the bottom of the vessel.

Processo de funcionamento
1The machine features an electrically controlled constant-speed stirring system, condenser and addition systems, and a jacket that requires connection to an external heating or cooling circulator.
2While stirring, hot or cold fluid is circulated through the jacket to maintain constant-temperature heating or cooling of the material inside.
3During heating reactions, vacuum conditions (external vacuum unit required) improve evaporation efficiency.
4Solvent vapour condenses in the glass condenser coil into liquid, which can either reflux back into the reactor or be recovered through the valve below the reflux elbow.
5When the reaction is complete, material can be discharged through the side outlet at the bottom of the vessel.

Especificações técnicas

Especificações da variante: SED-50BLFY-A

Especificações

Modelo
SED-50BLFY-A
Tensão
220V/50Hz
Utilidades
220V / 50Hz; total power 160 W. Requires external vacuum unit and external heating/cooling circulator.
Potência
0.16 kW
Pressão de ar
0.098MPa (vacuum)

Dimensões

Comprimento
750 mm
Largura
950 mm
Altura
2950 mm
Peso
148 kg
Área de instalação
750 × 950 × 2320 mm (W × D × H, lowered); 750 × 950 × 2950 mm (raised). Net weight 148 kg. Packing: 2380 × 680 × 1080 mm wooden crate, 1.75 m³, packed weight 225 kg.

Materiais

Materiais de contato
Borosilicate glass (expansion coefficient 3.3); PTFE (polytetrafluoroethylene); 304 aço inoxidável
Materiais do corpo
Square-steel anti-corrosion powder-coated main frame; aluminium alloy; aço inoxidável; PTFE reactor lid

Características principais

Vessel capacity 50 L (ID 365 mm, OD 410 mm, inner length 576 mm); jacket ~16 L
Electrically powered lid lift; stroke 740 mm
Vessel rotates 150° left via handwheel for direct pour discharge and easy cleaning
Stirring speed 0–450 rpm (variable frequency drive)
Vessel temperature range -80 °C to +250 °C
Vacuum capability 0.098 MPa
Temperature measurement accuracy ±1 °C (PT100 sensor)
Lid (Φ265 mm, 6-port, PTFE): stirring port Φ50 mm threaded, condenser/reflux port 50# ground glass, constant-pressure addition funnel port 40# standard, vacuum port 34# standard, temperature port 24# standard, solid addition port Φ80 mm threaded (ID 50 mm)
Dual-display variable-frequency speed controller (digital readout for speed and material temperature)
Crescent impeller Φ17 × 1000 H mm, blade span 190 mm; 304 SS + PTFE
Condenser Φ120 × 600 H mm, cooling area 0.5 m², lower Φ60 flange
Constant-pressure addition funnel 2 L
Discharge port: Φ75 mm flange, Φ33 mm bore, side-angled outlet, 290 mm above ground
Stirring and lifting fuse safety protection
Bottom-mounted braked swivel casters for mobility
Lift-and-rotate design: lid lifts, stirring shaft clears vessel, vessel rotates 150° for direct material pour-out and easy cleaning
All product-contact parts made of borosilicate glass (expansion coefficient 3.3) and PTFE — chemically inert and safe
Glass + PTFE side-discharge valve: no liquid pooling, fast solvent recovery
Buffer device on jacket inlet/outlet (SS flexible hose) protects glass fittings from pressure damage
Ceramic bearing + mechanical seal on stirring system: no contamination from shaft wear debris; high-temperature and wear resistant
High stirring and lifting fuse protection
Full-machine mobility via braked swivel casters

Aplicações

Chemical synthesis under vacuum and controlled temperature
Pharmaceutical intermediate and API synthesis
Solvent recovery and reflux reactions
Laboratory R&D reactions requiring controlled heating/cooling

Setores

Pharmaceutical R&D and manufacturing
Chemical synthesis
Laboratory research
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Documentação

Ficha técnica (PDF)
Visão geral do equipamento, especificações e dimensões · Documento original (inglês)
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Manual do operador
Instalação, operação e diagnóstico · Documento original (inglês)
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Folha comparativa (Padrão e Econômica)
Comparação das configurações · Documento original (inglês)
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Protocolos IQ / OQ / PQ
Documentação de validação para conformidade GMP · Documento original (inglês)
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Protocolos FAT / SAT
Testes de aceitação na fábrica e no local · Documento original (inglês)
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Desenhos CAD (STEP / IGES / DWG)
Desenhos de engenharia para a instalação · Documento original (inglês)
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Certificados de calibração
Nível sonoro, resistência de terra, rigidez dielétrica e rugosidade · Documento original (inglês)
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DQ (qualificação do projeto)
Protocolo completo de qualificação do projeto · Documento original (inglês)
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Certificados de materiais
Composição do aço inoxidável 316L · Documento original (inglês)
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